TY - JOUR
T1 - (+)-(1S,5R,6R)-6-[(S)-1-Hydroxy-2-(methoxymethyloxy)ethyl] -1-methyl-3-trichloromethyl-2-aza-4,7-dioxabicyclo[3.3.0]oct-2-en-8-one
AU - Oishi, Takeshi
AU - Oishi, Hiroki
AU - Tsuzaki, Syun
AU - Sato, Takaaki
AU - Chida, Noritaka
PY - 2012/11
Y1 - 2012/11
N2 - In the title compound, C11H14Cl3NO6, the fused five-membered oxazoline and tetrahydrofuran rings are essentially planar with maximum deviations of 0.069(1) and 0.031(1)Å, respectively, and make a dihedral angle of 64.23(11)°with each other. In the crystal, molecules are linked by O-H⋯O and C-H⋯O hydrogen bonds, forming chains along the b-axis direction. Further C-H⋯O hydrogen bonds are observed between the chains.
AB - In the title compound, C11H14Cl3NO6, the fused five-membered oxazoline and tetrahydrofuran rings are essentially planar with maximum deviations of 0.069(1) and 0.031(1)Å, respectively, and make a dihedral angle of 64.23(11)°with each other. In the crystal, molecules are linked by O-H⋯O and C-H⋯O hydrogen bonds, forming chains along the b-axis direction. Further C-H⋯O hydrogen bonds are observed between the chains.
KW - R factor = 0.027
KW - T = 90 K
KW - data-to-parameter ratio = 12.2
KW - mean ̄(C-C) = 0.003 Å
KW - single-crystal X-ray study
KW - wR factor = 0.069
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U2 - 10.1107/S1600536812042912
DO - 10.1107/S1600536812042912
M3 - Article
C2 - 23284496
AN - SCOPUS:84870948803
SN - 1600-5368
VL - 68
SP - o3185
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 11
ER -