TY - JOUR
T1 - (+)-3-{(4S,5S)-5-[1,1-dimethyl-2-(phenylthio)ethyl]-2,2-dimethyl-1,3-dioxolan-4-yl}prop-2-yn-1-ol
AU - Hosomi, Hiroyuki
AU - Ohba, Shigeru
AU - Ohmori, Ken
AU - Obitsu, Tetsuo
AU - Ogawa, Yasuyuki
AU - Ishikawa, Yuichi
AU - Yamamura, Shosuke
AU - Nishiyama, Shigeru
PY - 2000/1/1
Y1 - 2000/1/1
N2 - The absolute configuration was determined for the title compound. It was prepared in a synthetic study on the natural products, bryostatins. There were 163 Friedel pairs, which were not averaged. The completeness of symmetry unique reactions was 93.3%, which was due to the blind region of the low temperature apparatus. The hydroxyl H atom was located from a difference synthesis. The absolute structure was determined based on a Flack parameter value of 0.03 (3).
AB - The absolute configuration was determined for the title compound. It was prepared in a synthetic study on the natural products, bryostatins. There were 163 Friedel pairs, which were not averaged. The completeness of symmetry unique reactions was 93.3%, which was due to the blind region of the low temperature apparatus. The hydroxyl H atom was located from a difference synthesis. The absolute structure was determined based on a Flack parameter value of 0.03 (3).
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U2 - 10.1107/S0108270100003371
DO - 10.1107/S0108270100003371
M3 - Article
AN - SCOPUS:84924985434
VL - 56
SP - e142-e143
JO - Acta Crystallographica Section C: Crystal Structure Communications
JF - Acta Crystallographica Section C: Crystal Structure Communications
SN - 0108-2701
IS - 4
ER -