Abstract
The absolute configuration was determined for the title compound. It was prepared in a synthetic study on the natural products, bryostatins. There were 163 Friedel pairs, which were not averaged. The completeness of symmetry unique reactions was 93.3%, which was due to the blind region of the low temperature apparatus. The hydroxyl H atom was located from a difference synthesis. The absolute structure was determined based on a Flack parameter value of 0.03 (3).
| Original language | English |
|---|---|
| Pages (from-to) | e142-e143 |
| Journal | Acta Crystallographica Section C: Crystal Structure Communications |
| Volume | 56 |
| Issue number | 4 |
| Publication status | Published - 2000 |
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ASJC Scopus subject areas
- Biochemistry, Genetics and Molecular Biology(all)
Cite this
(+)-3-{(4S,5S)-5-[1,1-dimethyl-2-(phenylthio)ethyl]-2,2-dimethyl-1,3-dioxolan-4-yl}prop-2-yn-1-ol. / Hosomi, Hiroyuki; Ohba, Shigeru; Ohmori, Ken; Obitsu, Tetsuo; Ogawa, Yasuyuki; Ishikawa, Yuichi; Yamamura, Shosuke; Nishiyama, Shigeru.
In: Acta Crystallographica Section C: Crystal Structure Communications, Vol. 56, No. 4, 2000, p. e142-e143.Research output: Contribution to journal › Article
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TY - JOUR
T1 - (+)-3-{(4S,5S)-5-[1,1-dimethyl-2-(phenylthio)ethyl]-2,2-dimethyl-1,3-dioxolan-4-yl}prop-2-yn-1-ol
AU - Hosomi, Hiroyuki
AU - Ohba, Shigeru
AU - Ohmori, Ken
AU - Obitsu, Tetsuo
AU - Ogawa, Yasuyuki
AU - Ishikawa, Yuichi
AU - Yamamura, Shosuke
AU - Nishiyama, Shigeru
PY - 2000
Y1 - 2000
N2 - The absolute configuration was determined for the title compound. It was prepared in a synthetic study on the natural products, bryostatins. There were 163 Friedel pairs, which were not averaged. The completeness of symmetry unique reactions was 93.3%, which was due to the blind region of the low temperature apparatus. The hydroxyl H atom was located from a difference synthesis. The absolute structure was determined based on a Flack parameter value of 0.03 (3).
AB - The absolute configuration was determined for the title compound. It was prepared in a synthetic study on the natural products, bryostatins. There were 163 Friedel pairs, which were not averaged. The completeness of symmetry unique reactions was 93.3%, which was due to the blind region of the low temperature apparatus. The hydroxyl H atom was located from a difference synthesis. The absolute structure was determined based on a Flack parameter value of 0.03 (3).
UR - http://www.scopus.com/inward/record.url?scp=84924985434&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=84924985434&partnerID=8YFLogxK
M3 - Article
VL - 56
SP - e142-e143
JO - Acta Crystallographica Section C: Crystal Structure Communications
JF - Acta Crystallographica Section C: Crystal Structure Communications
SN - 0108-2701
IS - 4
ER -