TY - JOUR
T1 - A small-angle X-ray camera using a two-dimensional multiwire proportional chamber
AU - Furuno, T.
AU - Sasabe, H.
AU - Ikegami, A.
N1 - Funding Information:
The authors express thanks to Dr K. Kinosita Jr and Dr T. Kouyama of the Institute of Physical and Chemical Research for their support in constructing the two-dimensional X-ray system and suggestions in experiments. This work was supported by special coordination funds for promoting science and technology and a grant for 'Solar Energy Photosynthesis' given by the Agency of Science and Technology, Japan.
Publisher Copyright:
© 1987, Wiley-Blackwell. All rights reserved.
PY - 1987
Y1 - 1987
N2 - The construction and performance of a small-angle X-ray camera equipped with a two-dimensional multiwire proportional chamber (two-dimensional MWPC) are described. The system has been used for studies of the structure of biological samples with a conventional rotating-anode X-ray source. The small-angle camera is of Franks type with two orthogonal platinum-coated bent optical flats placed in a helium-tight box. The specimen-to-detector distance is variable between 60 and 260 cm. The sensitive area of the two-dimensional MWPC is 256 × 256 mm with 256 × 256 resolution elements. The camera covers high angles up to about 5 Å, although diffraction line widths in this region are highly broadened owing to parallax. The electronic system comprises NIM modules, a hand-made module and a commercially available compact two-dimensional multichannel analyser (two-dimensional MCA). The two-dimensional MCA has a memory size of 256 × 256 channels (24 bits/channel). The estimated dead time of this system is approximately 5 μs, which permits a maximum count rate of 20 kHz at 10% loss. Diffraction patterns of a Langmuir–Blodgett film of arachidic acid and stacked purple membranes and a solution scattering of horse spleen apoferritin are demonstrated as examples.
AB - The construction and performance of a small-angle X-ray camera equipped with a two-dimensional multiwire proportional chamber (two-dimensional MWPC) are described. The system has been used for studies of the structure of biological samples with a conventional rotating-anode X-ray source. The small-angle camera is of Franks type with two orthogonal platinum-coated bent optical flats placed in a helium-tight box. The specimen-to-detector distance is variable between 60 and 260 cm. The sensitive area of the two-dimensional MWPC is 256 × 256 mm with 256 × 256 resolution elements. The camera covers high angles up to about 5 Å, although diffraction line widths in this region are highly broadened owing to parallax. The electronic system comprises NIM modules, a hand-made module and a commercially available compact two-dimensional multichannel analyser (two-dimensional MCA). The two-dimensional MCA has a memory size of 256 × 256 channels (24 bits/channel). The estimated dead time of this system is approximately 5 μs, which permits a maximum count rate of 20 kHz at 10% loss. Diffraction patterns of a Langmuir–Blodgett film of arachidic acid and stacked purple membranes and a solution scattering of horse spleen apoferritin are demonstrated as examples.
UR - http://www.scopus.com/inward/record.url?scp=0006442185&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=0006442185&partnerID=8YFLogxK
U2 - 10.1107/S002188988708720X
DO - 10.1107/S002188988708720X
M3 - Article
AN - SCOPUS:0006442185
VL - 20
SP - 16
EP - 22
JO - Journal of Applied Crystallography
JF - Journal of Applied Crystallography
SN - 0021-8898
IS - 1
ER -