Amine-free silylation of alcohols under 4-methylpyridine N-oxide-catalyzed conditions

Keisuke Yoshida; Yuta Fujino; Yukihiro Itatsu; Hiroki Inoue; Yohei Kanoko; Ken Ichi Takao

doi:10.1016/j.tetlet.2015.12.114

Amine-free silylation of alcohols under 4-methylpyridine N-oxide-catalyzed conditions

Keisuke Yoshida, Yuta Fujino, Yukihiro Itatsu, Hiroki Inoue, Yohei Kanoko, Ken Ichi Takao

Department of Applied Chemistry

Research output: Contribution to journal › Article › peer-review

11 Citations (Scopus)

Abstract

Amine-free silylation of various alcohols catalyzed by 4-methylpyridine N-oxide in the presence of MS4A at room temperature was developed. This simple method gave various silyl ethers in a high yield.

Original language	English
Pages (from-to)	627-631
Number of pages	5
Journal	Tetrahedron Letters
Volume	57
Issue number	5
DOIs	https://doi.org/10.1016/j.tetlet.2015.12.114
Publication status	Published - 2016 Feb 3

Keywords

4-Methylpyridine N-oxide
Amine-free
MS4A
Silylation

ASJC Scopus subject areas

Biochemistry
Drug Discovery
Organic Chemistry

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10.1016/j.tetlet.2015.12.114

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title = "Amine-free silylation of alcohols under 4-methylpyridine N-oxide-catalyzed conditions",

abstract = "Amine-free silylation of various alcohols catalyzed by 4-methylpyridine N-oxide in the presence of MS4A at room temperature was developed. This simple method gave various silyl ethers in a high yield.",

keywords = "4-Methylpyridine N-oxide, Amine-free, MS4A, Silylation",

author = "Keisuke Yoshida and Yuta Fujino and Yukihiro Itatsu and Hiroki Inoue and Yohei Kanoko and Takao, {Ken Ichi}",

year = "2016",

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T1 - Amine-free silylation of alcohols under 4-methylpyridine N-oxide-catalyzed conditions

AU - Yoshida, Keisuke

AU - Fujino, Yuta

AU - Itatsu, Yukihiro

AU - Inoue, Hiroki

AU - Kanoko, Yohei

AU - Takao, Ken Ichi

PY - 2016/2/3

Y1 - 2016/2/3

N2 - Amine-free silylation of various alcohols catalyzed by 4-methylpyridine N-oxide in the presence of MS4A at room temperature was developed. This simple method gave various silyl ethers in a high yield.

AB - Amine-free silylation of various alcohols catalyzed by 4-methylpyridine N-oxide in the presence of MS4A at room temperature was developed. This simple method gave various silyl ethers in a high yield.

KW - 4-Methylpyridine N-oxide

KW - Amine-free

KW - MS4A

KW - Silylation

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DO - 10.1016/j.tetlet.2015.12.114

M3 - Article

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JF - Tetrahedron Letters

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ER -

Amine-free silylation of alcohols under 4-methylpyridine N-oxide-catalyzed conditions

Abstract

Keywords

ASJC Scopus subject areas

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