TY - JOUR
T1 - Crystal structure of 1-[4-(2,2-diphenylacetyl)piperazin-1-yl]-3-buten-2-ol
AU - Miyata, Yoshiyuki
AU - Osa, Yumiko
AU - Sato, Yoko
AU - Takino, Kouichi
AU - Kobayashi, Seiki
AU - Takeuchi, Tutomu
AU - Takayanagi, Hiroaki
N1 - Copyright:
Copyright 2018 Elsevier B.V., All rights reserved.
PY - 2004
Y1 - 2004
N2 - 1-[4-(2,2-Diphenylacetyl)piperazin-1-yl]-3-buten-2-ol (1) crystallizes in the monoclinic space group P21/a with a = 18.057(1), b = 6.036(2), c = 19.309(1)Å, β = 115.630(4)°, V = 1897.3(5)Å3, Z = 4. The carbonyl group and the nitrogen of piperazine constitutes an almost planar amide moiety due to being conjugated with the carbonyl group. An intermolecular hydrogen interaction of the hydroxyl group to another nitrogen of piperazine (bond distance: 2.86(3)Å) is present. 2004
AB - 1-[4-(2,2-Diphenylacetyl)piperazin-1-yl]-3-buten-2-ol (1) crystallizes in the monoclinic space group P21/a with a = 18.057(1), b = 6.036(2), c = 19.309(1)Å, β = 115.630(4)°, V = 1897.3(5)Å3, Z = 4. The carbonyl group and the nitrogen of piperazine constitutes an almost planar amide moiety due to being conjugated with the carbonyl group. An intermolecular hydrogen interaction of the hydroxyl group to another nitrogen of piperazine (bond distance: 2.86(3)Å) is present. 2004
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U2 - 10.2116/analscix.20.x33
DO - 10.2116/analscix.20.x33
M3 - Comment/debate
AN - SCOPUS:70450279107
SN - 1348-2238
VL - 20
SP - x33-x34
JO - Analytical Sciences: X-ray Structure Analysis Online
JF - Analytical Sciences: X-ray Structure Analysis Online
IS - 2
ER -