Formation of B-C-N ceramics investigated by emanation thermal analysis, TG and DTA

T. Sato; M. Hubáček; V. Balek; J. Šubrt; O. Kriz; T. Mitsuhashi

doi:10.1023/A:1010171710621

Formation of B-C-N ceramics investigated by emanation thermal analysis, TG and DTA

T. Sato, M. Hubáček, V. Balek, J. Šubrt, O. Kriz, T. Mitsuhashi

Research output: Contribution to journal › Article › peer-review

Abstract

Processes taking place during formation of B-C-N ceramics by thermal treatment of organic precursors were investigated using emanation thermal analysis (ETA), differential thermal analysis (DTA) and thermogravimetry (TG). An additional information about thermal behavior of precursors used for preparation of BC₄N, BN and CN_x ceramic systems by heating in argon up to 1100°C was obtained. The ETA enabled us to characterize microstructure changes in the samples at in situ conditions of thermal treatment. A good agreement of ETA, TG and DTA results was found.

Original language	English
Pages (from-to)	661-665
Number of pages	5
Journal	Journal of Thermal Analysis and Calorimetry
Volume	60
Issue number	2
DOIs	https://doi.org/10.1023/A:1010171710621
Publication status	Published - 2000 Jan 1
Externally published	Yes

ASJC Scopus subject areas

Condensed Matter Physics
Physical and Theoretical Chemistry

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abstract = "Processes taking place during formation of B-C-N ceramics by thermal treatment of organic precursors were investigated using emanation thermal analysis (ETA), differential thermal analysis (DTA) and thermogravimetry (TG). An additional information about thermal behavior of precursors used for preparation of BC4N, BN and CNx ceramic systems by heating in argon up to 1100°C was obtained. The ETA enabled us to characterize microstructure changes in the samples at in situ conditions of thermal treatment. A good agreement of ETA, TG and DTA results was found.",

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AU - Sato, T.

AU - Hubáček, M.

AU - Balek, V.

AU - Šubrt, J.

AU - Kriz, O.

AU - Mitsuhashi, T.

PY - 2000/1/1

Y1 - 2000/1/1

N2 - Processes taking place during formation of B-C-N ceramics by thermal treatment of organic precursors were investigated using emanation thermal analysis (ETA), differential thermal analysis (DTA) and thermogravimetry (TG). An additional information about thermal behavior of precursors used for preparation of BC4N, BN and CNx ceramic systems by heating in argon up to 1100°C was obtained. The ETA enabled us to characterize microstructure changes in the samples at in situ conditions of thermal treatment. A good agreement of ETA, TG and DTA results was found.

AB - Processes taking place during formation of B-C-N ceramics by thermal treatment of organic precursors were investigated using emanation thermal analysis (ETA), differential thermal analysis (DTA) and thermogravimetry (TG). An additional information about thermal behavior of precursors used for preparation of BC4N, BN and CNx ceramic systems by heating in argon up to 1100°C was obtained. The ETA enabled us to characterize microstructure changes in the samples at in situ conditions of thermal treatment. A good agreement of ETA, TG and DTA results was found.

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Formation of B-C-N ceramics investigated by emanation thermal analysis, TG and DTA

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