Homogenization and Particle Size Reduction of PbTiO3 by Ball-Milling of Precursor Gels

Katsuhiko Takeuchi, Tetsuhiko Isobe, Mamoru Senna

Research output: Contribution to journalArticle

10 Citations (Scopus)

Abstract

Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO3 obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.

Original languageEnglish
Pages (from-to)401-405
Number of pages5
JournalJournal of Solid State Chemistry
Volume109
Issue number2
DOIs
Publication statusPublished - 1994 Apr

Fingerprint

alkoxides
Ball milling
homogenizing
Calcination
Oxides
balls
Gels
Particle size
Heat treatment
gels
Air
Chemical analysis
chemical analysis
roasting
oxides
high resolution
air

ASJC Scopus subject areas

  • Materials Chemistry
  • Physical and Theoretical Chemistry
  • Inorganic Chemistry

Cite this

Homogenization and Particle Size Reduction of PbTiO3 by Ball-Milling of Precursor Gels. / Takeuchi, Katsuhiko; Isobe, Tetsuhiko; Senna, Mamoru.

In: Journal of Solid State Chemistry, Vol. 109, No. 2, 04.1994, p. 401-405.

Research output: Contribution to journalArticle

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