Homogenization and particle size reduction of PbTiO3 by ball-milling of precursor gels

Katsuhiko Takeuchi, Tetsuhiko Isobe, Mamoru Senna

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10 Citations (Scopus)

Abstract

Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO3 obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.

Original languageEnglish
Pages (from-to)401-405
Number of pages5
JournalJournal of Solid State Chemistry
Volume109
Issue number2
DOIs
Publication statusPublished - 1994 Apr

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ASJC Scopus subject areas

  • Electronic, Optical and Magnetic Materials
  • Ceramics and Composites
  • Condensed Matter Physics
  • Physical and Theoretical Chemistry
  • Inorganic Chemistry
  • Materials Chemistry

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