Microwave-assisted rapid synthesis of anatase TiO2 nanosized particles in an ionic liquid-water system

Ayami Suzuki; Hideki Yamaguchi; Hiroyuki Kageyama; Yuya Oaki; Hiroaki Imai

doi:10.2109/jcersj2.123.79

Microwave-assisted rapid synthesis of anatase TiO₂ nanosized particles in an ionic liquid-water system

Ayami Suzuki, Hideki Yamaguchi, Hiroyuki Kageyama, Yuya Oaki, Hiroaki Imai

Department of Applied Chemistry

Research output: Contribution to journal › Article › peer-review

6 Citations (Scopus)

Abstract

Nanosized anatase TiO₂ crystals were rapidly prepared in a mixture of an ionic liquid (1-butyl-3-methylimidazolium chloride) and water under microwave irradiation for 5min. The crystal size in the c axis was varied in the range from ∼5 to ∼17nm with prolongation of the irradiation time. A high susceptibility of the ionic liquid to microwave and a catalytic property of the imidazolium cation are effective for the rapid synthesis of the highly crystalline nanosized particles.

Original language	English
Pages (from-to)	79-82
Number of pages	4
Journal	Journal of the Ceramic Society of Japan
Volume	123
Issue number	1434
DOIs	https://doi.org/10.2109/jcersj2.123.79
Publication status	Published - 2015 Jan 1

Keywords

IL
Nanoparticle
Size control
Titanium dioxide

ASJC Scopus subject areas

Ceramics and Composites
Chemistry(all)
Condensed Matter Physics
Materials Chemistry

Access to Document

10.2109/jcersj2.123.79

Cite this

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title = "Microwave-assisted rapid synthesis of anatase TiO2 nanosized particles in an ionic liquid-water system",

abstract = "Nanosized anatase TiO2 crystals were rapidly prepared in a mixture of an ionic liquid (1-butyl-3-methylimidazolium chloride) and water under microwave irradiation for 5min. The crystal size in the c axis was varied in the range from ∼5 to ∼17nm with prolongation of the irradiation time. A high susceptibility of the ionic liquid to microwave and a catalytic property of the imidazolium cation are effective for the rapid synthesis of the highly crystalline nanosized particles.",

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author = "Ayami Suzuki and Hideki Yamaguchi and Hiroyuki Kageyama and Yuya Oaki and Hiroaki Imai",

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T1 - Microwave-assisted rapid synthesis of anatase TiO2 nanosized particles in an ionic liquid-water system

AU - Suzuki, Ayami

AU - Yamaguchi, Hideki

AU - Kageyama, Hiroyuki

AU - Oaki, Yuya

AU - Imai, Hiroaki

PY - 2015/1/1

Y1 - 2015/1/1

N2 - Nanosized anatase TiO2 crystals were rapidly prepared in a mixture of an ionic liquid (1-butyl-3-methylimidazolium chloride) and water under microwave irradiation for 5min. The crystal size in the c axis was varied in the range from ∼5 to ∼17nm with prolongation of the irradiation time. A high susceptibility of the ionic liquid to microwave and a catalytic property of the imidazolium cation are effective for the rapid synthesis of the highly crystalline nanosized particles.

AB - Nanosized anatase TiO2 crystals were rapidly prepared in a mixture of an ionic liquid (1-butyl-3-methylimidazolium chloride) and water under microwave irradiation for 5min. The crystal size in the c axis was varied in the range from ∼5 to ∼17nm with prolongation of the irradiation time. A high susceptibility of the ionic liquid to microwave and a catalytic property of the imidazolium cation are effective for the rapid synthesis of the highly crystalline nanosized particles.

KW - IL

KW - Nanoparticle

KW - Size control

KW - Titanium dioxide

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