Preparation and characterization of monodisperse FePd nanoparticles

Yanglong Hou, Hiroshi Kondoh, Toshihiro Kogure, Toshiaki Ohta

Research output: Contribution to journalArticle

65 Citations (Scopus)

Abstract

Monodisperse FePd nanoparticles were prepared by polyol reduction of palladium acetylacetonate and thermal decomposition of iron pentacarbonyl, using a combination of n-adamantanecarboxylic acid and tri-alkylphosphine as stabilizers. The mean particle size can be tuned from 11 to 16 nm by controlling the concentration and type of stabilizers and reaction conditions. High monodispersity of FePd nanoparticles leads to the formation of two-dimensional (2D) superlattices consisting of hexagonal close-packed particles, which was confirmed by X-ray diffraction pattern and high-resolution transmission electron microscopic (HRTEM) images. This route provides a promising candidate for studying the magnetic properties of nanosized FePd materials.

Original languageEnglish
Pages (from-to)5149-5152
Number of pages4
JournalChemistry of Materials
Volume16
Issue number24
Publication statusPublished - 2004 Nov 30
Externally publishedYes

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Nanoparticles
Polyols
Superlattices
Palladium
Diffraction patterns
Magnetic properties
Pyrolysis
Particle size
Iron
X ray diffraction
Acids
Electrons
polyol
adamantanecarboxylic acid
acetyl acetonate
iron pentacarbonyl

ASJC Scopus subject areas

  • Materials Chemistry
  • Materials Science(all)

Cite this

Preparation and characterization of monodisperse FePd nanoparticles. / Hou, Yanglong; Kondoh, Hiroshi; Kogure, Toshihiro; Ohta, Toshiaki.

In: Chemistry of Materials, Vol. 16, No. 24, 30.11.2004, p. 5149-5152.

Research output: Contribution to journalArticle

Hou, Y, Kondoh, H, Kogure, T & Ohta, T 2004, 'Preparation and characterization of monodisperse FePd nanoparticles', Chemistry of Materials, vol. 16, no. 24, pp. 5149-5152.
Hou, Yanglong ; Kondoh, Hiroshi ; Kogure, Toshihiro ; Ohta, Toshiaki. / Preparation and characterization of monodisperse FePd nanoparticles. In: Chemistry of Materials. 2004 ; Vol. 16, No. 24. pp. 5149-5152.
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