Crystal structure of (-)-methyl (R,E)-4-[(2R,4R)-2-Amino-2-Trichloromethyl-1,3-dioxolan-4-yl]-4-hydroxy-2-methylbut-2-enoate Oishi Takeshi

Takeshi Oishi, Mayu Kidena, Tomoya Sugai, Takaaki Satou, Noritaka Chida

研究成果: Article

抜粋

In the title compound, C10H14Cl3NO5, the five-membered dioxolane ring adopts an envelope conformation with the C atom bonded to the butenoate side chain as the flap. It deviates from the mean plane of the other atoms in the ring by 0.446 (6) Å. In the crystal, molecules are connected by O-H·O hydrogen bonds into helical chains running along the b-Axis direction. The chains are linked into a sheet structure parallel to (001) by an N-H·O hydrogen bond. These classical hydrogen bonds enclose an R 4 4 (24) graph-set motif in the sheet structure. Furthermore, a weak intermolecular C-H·Cl interaction expands the sheet structures into a three-dimensional network.

元の言語English
ページ(範囲)983-986
ページ数4
ジャーナルActa Crystallographica Section E: Crystallographic Communications
73
DOI
出版物ステータスPublished - 2017

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ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)
  • Condensed Matter Physics

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