TY - JOUR
T1 - Homogenization and particle size reduction of PbTiO3 by ball-milling of precursor gels
AU - Takeuchi, Katsuhiko
AU - Isobe, Tetsuhiko
AU - Senna, Mamoru
PY - 1994/4
Y1 - 1994/4
N2 - Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO3 obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.
AB - Ball-milling of mixed gel derived from a simple mixing of component alkoxides increased the compositional microhomogeneity, judged quantitatively by high-resolution microprobe chemical analysis. At the same time, the particle size of PbTiO3 obtained after calcination at 1023 K for 2 hr in air decreased, approaching those of oxide fine particles delivered from a bidentate alkoxide through an identical thermal treatment.
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U2 - 10.1006/jssc.1994.1119
DO - 10.1006/jssc.1994.1119
M3 - Article
AN - SCOPUS:0011486792
VL - 109
SP - 401
EP - 405
JO - Journal of Solid State Chemistry
JF - Journal of Solid State Chemistry
SN - 0022-4596
IS - 2
ER -