Hydrothermal synthesis of hydroxyapatite from octacalcium phosphate: Effect of hydrothermal temperature

Masanobu Kamitakahara, Natsuko Ito, Setsuaki Murakami, Noriaki Watanabe, Koji Ioku

研究成果: Article

22 引用 (Scopus)

抜粋

Hydroxyapatite (HA) was synthesized by the hydrothermal treatment of octacalcium phosphate (OCP). Powder of OCP was hydrothermally treated with distilled water at 120-240°C for 3-24 h. Only diffraction lines assigned to HA were detected by X-ray diffraction (XRD) even after the treatment at 120°C for 3 h. The crystallinity of the formed HA increased with increasing the treatment temperature and period. Plate-shaped particles were split into small strip-shaped particles by the hydrothermal treatment and this phenomenon was obvious when the treatment temperature was high and the period was long. However, the plate-shape morphology was remained when OCP was transformed to HA at 120°C for 3 h. The hydrothermal treatment of OCP is useful to synthesize the plate-shaped HA particles in a short period.

元の言語English
ページ(範囲)385-387
ページ数3
ジャーナルJournal of the Ceramic Society of Japan
117
発行部数1363
DOI
出版物ステータスPublished - 2009 3
外部発表Yes

ASJC Scopus subject areas

  • Ceramics and Composites
  • Chemistry(all)
  • Condensed Matter Physics
  • Materials Chemistry

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